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Beilstein J. Org. Chem. 2021, 17, 2385–2389, doi:10.3762/bjoc.17.155
Graphical Abstract
Scheme 1: Dimerisation of α-lithio epoxides or aziridines [3-5].
Scheme 2: Proposed eliminative cross-coupling of carbenoids to allylic alcohols (X = O) or allylic amines (X ...
Scheme 3: Allylic alcohol 6 by one-carbon homologation from epoxide 5.
Scheme 4: Internal allylic alcohols from epoxides and stannane 7.
Scheme 5: Cyclopropylidene synthesis from epoxide 5.
Scheme 6: Synthesis of vinylsilane 14.
Scheme 7: Allylic alcohol 8 from epoxide 5 and sulfone 15.
Scheme 8: Allylic amines from aziridine 17.
Scheme 9: Cyclopropylidene synthesis from aziridine 20.
Scheme 10: Cinnamylamine 23 synthesis from aziridine 17.
Scheme 11: Cinnamylamine 23 synthesis from isopropyl or neopentyl benzylic ethers 26 and 27.